Synthesis and reduction of thieno[2′,3′(3′,2′ or 3′,4′):5,6]‐azocino[2,1‐a]isoindole‐7, 13‐diones
Identifieur interne : 001229 ( France/Analysis ); précédent : 001228; suivant : 001230Synthesis and reduction of thieno[2′,3′(3′,2′ or 3′,4′):5,6]‐azocino[2,1‐a]isoindole‐7, 13‐diones
Auteurs : Mohamed Othman [France] ; Pascal Pigeon [France] ; Bernard Decroix [France]Source :
- Journal of Heterocyclic Chemistry [ 0022-152X ] ; 1998-11.
Abstract
A synthesis of the thieno[2′,3′(3′,2′ or 3′,4′):5,6]azocino[2,1‐a]isoindole‐7,13‐diones 6a‐c was developed from N‐thienylethylphthalimides 3a‐c using a Wittig reaction followed by a Friedel‐Crafts cyclization of acetic acid derivatives 5a‐c. Reduction of ketones 6a‐c into alcohols 7a‐c was stereo specific.
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DOI: 10.1002/jhet.5570350635
Affiliations:
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<front><div type="abstract">A synthesis of the thieno[2′,3′(3′,2′ or 3′,4′):5,6]azocino[2,1‐a]isoindole‐7,13‐diones 6a‐c was developed from N‐thienylethylphthalimides 3a‐c using a Wittig reaction followed by a Friedel‐Crafts cyclization of acetic acid derivatives 5a‐c. Reduction of ketones 6a‐c into alcohols 7a‐c was stereo specific.</div>
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